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1 article(s) from Kontaxis, Georg

Synthesis of fluorinated maltose derivatives for monitoring protein interaction by ¹⁹F NMR

Michaela Braitsch,
Hanspeter Kählig,
Georg Kontaxis,
Michael Fischer,
Toshinari Kawada,
Robert Konrat and
Walther Schmid

Beilstein J. Org. Chem. 2012, 8, 448–455, doi:10.3762/bjoc.8.51

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Graphical Abstract

Figure 1: Schematic diagram of the network of hydrogen bonds in the binding pocket of the complex between MBP...

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Figure 2: 2-¹⁹F-Maltose reporter system: Nonstereoselective fluorine labeling at the 2-position of maltose le...

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Scheme 1: Syntheses of maltose derivatives; reagents and conditions: (a) Ac₂O, Pyr, 97%; (b) HBr, AcOH, 99%; ...

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Scheme 2: Synthesis of the maltose- and galacto-type derivatives; reagents and conditions: (a) TBDMS-Cl, imid...

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Figure 3: 1-D ¹⁹F NMR: Experimental demonstration of differential binding of gluco- and manno-type 2-F-labele...

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Figure 4: ¹⁹F NMR expansion (of Figure 3) of the gluco-type region of the 2-F-maltose reporter system.

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Figure 5: Competitive titration with the 2-F-maltose reporter system and ¹⁹F NMR: only the important section ...

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Published 27 Mar 2012

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Synthesis of fluorinated maltose derivatives for monitoring protein interaction by 19F NMR

Synthesis of fluorinated maltose derivatives for monitoring protein interaction by ¹⁹F NMR